(S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide

Base Information

• Chemical Name: (S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide
• CAS No.: 1228108-64-2
• Molecular Formula: C₄₈H₅₂N₂O₈
• Molecular Weight: 784.949

Synonyms:(S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide

Chemical Property of (S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide

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Technology Process of (S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide

There total 1 articles about (S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthalene-5,5'-dicarboxylic acid (1173894-90-0) + (2S)-2-phenyl-1-propanamine (17596-79-1) → (S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N5,N5'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide (1228108-64-2)

Guidance literature:

1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthalene-5,5'-dicarboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

(2S)-2-phenyl-1-propanamine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jm1001265

Reference yield:

(S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N5,N5'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide (1228108-64-2) → (Ra)-1,1', 6,6',7,7'-hexahydroxy-3,3'-dimethyl-N5,N5'-bis((S)-2-phenylpropyl)-N5'-((S)-2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide + (Sa)-1,1', 6,6',7,7'-hexahydroxy-3,3'-dimethyl-N5,N5'-bis((S)-2-phenylpropyl)-N5'-((S)-2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide

Guidance literature:

(S,S)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-N₅,N₅'-bis(2-phenylpropyl)-2,2'-binaphthyl-5,5'-dicarboxamide; With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 3h;

With hydrogenchloride; water; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jm1001265

upstream raw materials:

1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthalene-5,5'-dicarboxylic acid

(2S)-2-phenyl-1-propanamine

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