6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene

Base Information

• Chemical Name: 6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene
• CAS No.: 307001-39-4
• Molecular Formula: C₁₇H₂₈O₃Si
• Molecular Weight: 308.493

Synonyms:6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene

Chemical Property of 6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene

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Technology Process of 6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene

There total 1 articles about 6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester (1026970-16-0) → 6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene (307001-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: pyridine; DMAP / 20 °C

With pyridine; dmap; lithium aluminium tetrahydride; In diethyl ether; 1: Reduction / 2: Acylation;

DOI:10.1021/jo000209v

Reference yield: 65.0%

6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene (307001-39-4) → 4-acetoxymethyl-4-(3'-butenyl)-3-methoxy-5-(trimethylsilyl)-2,5-cyclohexadien-1-one

Guidance literature:

With tert.-butylhydroperoxide; dipyridinium dichromate; Celite; In decane; benzene; at 20 ℃;

DOI:10.1021/jo000209v

upstream raw materials:

1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

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