1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

Base Information

Chemical Name:1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester
CAS No.:1026970-16-0
Molecular Formula:C₁₇H₂₈O₃Si
Molecular Weight:308.493
Hs Code.:

Synonyms:1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

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Chemical Property of 1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

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Technology Process of 1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

There total 1 articles about 1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5162-44-7
1-bromo-4-butene

: 190896-24-3
ethyl 2-methoxy-6-trimethylsilylbenzoate

: 1026970-16-0
1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

Guidance literature:: With penta-1,3-diene; ammonia; lithium; In tetrahydrofuran; tert-butyl alcohol; at -78 ℃; for 1h;
DOI:10.1021/jo000209v

Reference yield:

: 1026970-16-0
1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

: (1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienyl)-methanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1021/jo000209v

Reference yield:

: 1026970-16-0
1-but-3-enyl-2-methoxy-6-trimethylsilanyl-cyclohexa-2,5-dienecarboxylic acid ethyl ester

: 307001-39-4
6-acetoxymethyl-6-(3'-butenyl)-1-methoxy-4-(trimethylsilyl)-1,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: pyridine; DMAP / 20 °C

With pyridine; dmap; lithium aluminium tetrahydride; In diethyl ether; 1: Reduction / 2: Acylation;
DOI:10.1021/jo000209v