Technology Process of 3-(3-oxobutyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl acetate
There total 10 articles about 3-(3-oxobutyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
1,4-dioxane;
at 103 ℃;
for 16h;
DOI:10.1016/j.bmcl.2010.12.034
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N,N-dimethyl-formamide / 1 h / 80 °C
2: formic acid; water / 1 h / 100 °C
3: toluene / 1 h / 90 °C
4: 10% palladium on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C
5: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 16 h / 103 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; formic acid; 10% palladium on activated carbon; water; hydrogen; potassium acetate;
In
1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide; toluene;
3: Wittig reaction;
DOI:10.1016/j.bmcl.2010.12.034
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene / 1 h / 90 °C
2: 10% palladium on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 16 h / 103 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 10% palladium on activated carbon; hydrogen; potassium acetate;
In
1,4-dioxane; ethyl acetate; toluene;
1: Wittig reaction;
DOI:10.1016/j.bmcl.2010.12.034
