N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Base Information

Chemical Name:N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide
CAS No.:1237587-15-3
Molecular Formula:C₁₈H₁₄Cl₂F₃N₃O₂
Molecular Weight:432.229
Hs Code.:

Synonyms:N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

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Chemical Property of N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Chemical Property:

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Technology Process of N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

There total 11 articles about N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-14-2
tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 1237587-15-3
N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Guidance literature:: tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate; With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

Reference yield:

: tert-butyl N'-acetyl-N-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 1237587-15-3
N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 3431-62-7,20747-39-1
3-nitrobenzaldoxime

: 1237587-15-3
N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: acetic acid; iron / ethanol; water / 1.25 h / 20 - 75 °C

3.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

4.1: 4-dimethylpyridine / tetrahydrofuran / 1.5 h / 20 °C

5.1: sodium hydroxide; sodium hypochlorite; ammonia; ammonium chloride / Aliquat 336 / water; tert-butyl methyl ether / 12.33 h / 20 °C

6.1: triethylamine / tetrahydrofuran / 14 h / 0 - 20 °C

7.1: trifluoroacetic acid / tetrahydrofuran / 1 h / 20 °C

With sodium hypochlorite; N-chloro-succinimide; ammonia; iron; ammonium chloride; acetic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; Aliquat 336; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide;