methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

Base Information

Chemical Name:methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate
CAS No.:1370330-82-7
Molecular Formula:C₂₁H₁₈N₄O₆
Molecular Weight:422.397
Hs Code.:

Synonyms:methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

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Chemical Property of methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

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Technology Process of methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

There total 9 articles about methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.6%

: 205876-53-5
3-phenyl-4-(3-bromo-1-propyl)-Δ2-1,2,4-oxadiazolin-5-one

: C₁₀H₇N₂O₄^(1-)*K⁽¹⁺⁾

: 1370330-82-7
methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

Guidance literature:: In N,N-dimethyl-formamide; at 40 ℃; for 168h;
DOI:10.1002/jlcr.1954

Reference yield:

: 1456-22-0
3-phenyl-4H-[1,2,4]oxadiazol-5-one

: 1370330-82-7
methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / methanol / 1 h / 20 °C

2: N,N-dimethyl-formamide / 72 h / 20 °C

3: N,N-dimethyl-formamide / 168 h / 40 °C

With potassium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1954

Reference yield:

: 1129-35-7
4-cyanobenzoic acid methyl ester

: 1370330-82-7
methyl 4-(4,5-dihydro-5-oxo-4-(3-(5-oxo-3-phenyl-1,2,4-oxadiazol-4-yl)propyl)-1,2,4-oxadiazol-3-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 3.5 h / 20 - 90 °C

2: 1,4-dioxane / 0.5 h / 110 °C

3: potassium hydroxide / methanol / 1 h / 20 °C

4: N,N-dimethyl-formamide / 168 h / 40 °C

With hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium hydroxide; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1954