Technology Process of C17H21BrO2
There total 7 articles about C17H21BrO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bromine; silver trifluoroacetate;
In
chloroform;
for 3h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: mercury(II) oxide; bromine / 3.67 h / 80 °C
2: aluminum (III) chloride / 20 - 60 °C / Inert atmosphere; Cooling with ice
3: lithium hydroxide / tetrahydrofuran
4: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C
5: triethylamine / tetrahydrofuran; acetonitrile / 6 h / 0 - 20 °C
6: triethylamine; silver benzoate / 5 h / 20 °C / Sonication
7: bromine; silver trifluoroacetate / chloroform / 3 h
With
aluminum (III) chloride; oxalyl dichloride; bromine; silver trifluoroacetate; silver benzoate; triethylamine; N,N-dimethyl-formamide; mercury(II) oxide; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; chloroform; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hydroxide / tetrahydrofuran
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C
3: triethylamine / tetrahydrofuran; acetonitrile / 6 h / 0 - 20 °C
4: triethylamine; silver benzoate / 5 h / 20 °C / Sonication
5: bromine; silver trifluoroacetate / chloroform / 3 h
With
oxalyl dichloride; bromine; silver trifluoroacetate; silver benzoate; triethylamine; N,N-dimethyl-formamide; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; chloroform; acetonitrile;