1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline

Base Information

• Chemical Name: 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline
• CAS No.: 32039-37-5
• Molecular Formula: C₂₁H₂₇NO₅
• Molecular Weight: 373.449

Synonyms:1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline

Chemical Property of 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline

There total 4 articles about 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,6,7-trimethoxy-1-(3',4'-dimethoxybenzyl)3,4-dihydroisoquinoline (47539-89-9) → 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline (32039-37-5)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h;

DOI:10.1055/s-2001-15143

Reference yield:

(3,4-Dimethoxyphenyl)acetic acid (93-40-3) → 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline (32039-37-5)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃ / toluene / 3.5 h / 20 - 120 °C

2: NaBH₄ / methanol / 2.5 h / 20 °C

With sodium tetrahydroborate; trichlorophosphate; In methanol; toluene; 1: Bischler-Napieralski reaction;

DOI:10.1002/hlca.200490005

Reference yield:

mescaline (54-04-6) → 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline (32039-37-5)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃ / toluene / 3.5 h / 20 - 120 °C

2: NaBH₄ / methanol / 2.5 h / 20 °C

With sodium tetrahydroborate; trichlorophosphate; In methanol; toluene; 1: Bischler-Napieralski reaction;

DOI:10.1002/hlca.200490005

upstream raw materials:

5,6,7-trimethoxy-1-(3',4'-dimethoxybenzyl)3,4-dihydroisoquinoline

(3,4-Dimethoxyphenyl)acetic acid

mescaline

Downstream raw materials:

1-(3,4-dimethoxy-benzyl)-5,6,7-trimethoxy-3,4-dihydro-isoquinoline 2-oxide

14-(3,4-dimethoxyphenyl)-3-hydroxy-2,10,11,12-tetramethoxy-8,9-dihydro-6H-chromeno[4’,3’:4,5]pyrrolo[2,1-a]isoquinolin-6-one

2-(2,4-diisopropoxy-5-methoxy-phenyl)-1-(3,4-dimethoxy-phenyl)-7,8,9-trimethoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-3-carboxylic acid ethyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 32039-37-5 1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-5,6,7-trimethoxyisoquinoline

Send

Send

Metric Ton KG G Pound L ML

Send

Send