C₁₇H₂₆N₂O₇S

Base Information

• Chemical Name: C₁₇H₂₆N₂O₇S
• CAS No.: 765908-10-9
• Molecular Formula: C₁₇H₂₆N₂O₇S
• Molecular Weight: 402.469
• Mol file: 765908-10-9.mol

Synonyms:C₁₇H₂₆N₂O₇S

Chemical Property of C₁₇H₂₆N₂O₇S

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₇H₂₆N₂O₇S

There total 1 articles about C₁₇H₂₆N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-Epoxyhexane (1436-34-6) + N-(tert-butoxycarbonyl)-2-nitrobenzenesulfonamide (198572-71-3) → (R)-hexane-1,2-diol (84994-66-1) + C17H26N2O7S (765908-10-9)

Guidance literature:

1,2-Epoxyhexane; With water; (S,S)-[N,N-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexane-diamino]cobalt(III) acetate; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

N-(tert-butoxycarbonyl)-2-nitrobenzenesulfonamide; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1002/anie.200460369

Reference yield:

C17H26N2O7S (765908-10-9) → N-(2-hydroxy-hexyl)-2-nitro-benzenesulfonamide

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 1.5h;

DOI:10.1002/anie.200460369

Reference yield:

C17H26N2O7S (765908-10-9) → Methanesulfonic acid (S)-1-[(2-nitro-benzenesulfonylamino)-methyl]-pentyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: CF₃COOH / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: pyridine; DMAP / CH₂Cl₂ / 0.5 h / 20 °C

With pyridine; dmap; trifluoroacetic acid; In dichloromethane;

DOI:10.1002/anie.200460369

upstream raw materials:

1,2-Epoxyhexane

N-(tert-butoxycarbonyl)-2-nitrobenzenesulfonamide