benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

Base Information

Chemical Name:benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate
CAS No.:259093-34-0
Molecular Formula:C₂₇H₃₆N₂O₆
Molecular Weight:484.593
Hs Code.:

Synonyms:benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

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Chemical Property of benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

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Technology Process of benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

There total 5 articles about benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 197635-07-7
1-tert-butoxycarbonyl-1-methyl-2-sec-butyl-hydrazine

: C₁₇H₁₅ClO₄

: 259093-34-0
benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 21075-83-2
1-methyl-1-tert-butoxycarbonylhydrazine

: 259093-34-0
benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: propan-2-ol / Heating

2: NaCNBH₃; AcOH / methanol / 0 °C / pH 3 - 4

3: Et₃N / tetrahydrofuran / 12 h / 20 °C

With sodium cyanoborohydride; acetic acid; triethylamine; In tetrahydrofuran; methanol; isopropyl alcohol;
DOI:10.1021/jo001749v

Reference yield:

: 7622-21-1,93434-59-4,7622-22-2
(R)-benzyl mandelate

: 259093-34-0
benzyl 1-(2-tert-butoxycarbonyl-2-methyl-1-sec-butyl-hydrazyl)-carbonyloxy-2-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran; toluene / 0 - 20 °C

2: Et₃N / tetrahydrofuran / 12 h / 20 °C

With triethylamine; In tetrahydrofuran; toluene;
DOI:10.1021/jo001749v