2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

Base Information

Chemical Name:2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide
CAS No.:1610725-17-1
Molecular Formula:C₂₀H₂₆BrNO₃Si
Molecular Weight:436.421
Hs Code.:

Synonyms:2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

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Technology Process of 2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

There total 4 articles about 2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 111359-74-1
4-[(tert-butyldimethylsilyl)oxy]aniline

: 56658-04-9
2-bromo-5-methoxybenzoyl chloride

: 1610725-17-1
2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.04.047

Reference yield:

: 22921-68-2
2-bromo-5-methoxy-benzoic acid

: 1610725-17-1
2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Reflux

2: triethylamine / dichloromethane / 3 h / Inert atmosphere

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2014.04.047

Reference yield:

: 123-30-8
4-amino-phenol

: 1610725-17-1
2-bromo-N-(4-((tert-butyldimethylsilyl)oxy)phenyl)-5-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / tetrahydrofuran / 0.5 h / 20 °C

2: triethylamine / dichloromethane / 3 h / Inert atmosphere

With 1H-imidazole; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2014.04.047