4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

Base Information

Chemical Name:4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine
CAS No.:186347-39-7
Molecular Formula:C₂₁H₃₁N₃O₂
Molecular Weight:357.496
Hs Code.:

Synonyms:4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

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Chemical Property of 4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

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Technology Process of 4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

There total 4 articles about 4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 191328-20-8
4-cyano-4-(2-methylphenyl)piperidine

: 186347-39-7
4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

Guidance literature:: DOI:10.1016/S0960-894X(00)00307-3

Reference yield:

: 186347-30-8
4-cyano-4-(2-methylphenyl)piperidine hydrochloride

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 4-cyano-N-(3-[N-{1,1-dimethylethoxycarbonyl}]amino)4-(2-methylphenyl)propylpiperidine

: 186347-39-7
4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 186347-28-4
4-cyano-N-(1,1-dimethylethoxy)carbonyl-4-(2-methylphenyl)-piperidine

: 186347-39-7
4-cyano-4-(2-methylphenyl)-N-[3-{(1,1-dimethyl-ethoxy) carbonyl}amino]propyl piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / ethyl acetate / 0 °C

2: Et₃N / dimethylformamide / 23 °C

With hydrogenchloride; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(01)00320-1