2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

Base Information

Chemical Name:2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide
CAS No.:115152-49-3
Molecular Formula:C₁₇H₁₈BrClO₇
Molecular Weight:449.683
Hs Code.:

Synonyms:2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

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Chemical Property of 2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

Chemical Property:

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Technology Process of 2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

There total 3 articles about 2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104992-63-4
Methyl 4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 115152-49-3
2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / pyridine; CH₂Cl₂ / 1 h / 0 °C

2: 89 percent / pyridine; CH₂Cl₂ / 2 h / 0 °C

3: 1.) bromine, tetraethylammonium bromide / 1.) dichloromethane; dichloromethane, r.t., 3 h

With tetraethylammonium bromide; bromine; In pyridine; dichloromethane;
DOI:10.1016/0008-6215(88)80046-6

Reference yield:

: 115152-47-1
methyl 4,6-O-benzylidene-3-O-(chloroacetyl)-1-thio-β-D-galactopyranoside

: 115152-49-3
2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine; CH₂Cl₂ / 2 h / 0 °C

2: 1.) bromine, tetraethylammonium bromide / 1.) dichloromethane; dichloromethane, r.t., 3 h

With tetraethylammonium bromide; bromine; In pyridine; dichloromethane;
DOI:10.1016/0008-6215(88)80046-6

Reference yield:

: 115152-48-2
methyl 2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-1-thio-β-D-galactopyranoside

: 115152-49-3
2-O-acetyl-4,6-O-benzylidene-3-O-(chloroacetyl)-α-D-galactopyranosyl bromide

Guidance literature:: With tetraethylammonium bromide; bromine; Yield given. Multistep reaction; 1.) dichloromethane; dichloromethane, r.t., 3 h;
DOI:10.1016/0008-6215(88)80046-6