C₆₅H₈₂O₁₀SSi

Base Information

Chemical Name:C₆₅H₈₂O₁₀SSi
CAS No.:1294354-35-0
Molecular Formula:C₆₅H₈₂O₁₀SSi
Molecular Weight:1083.51
Hs Code.:

C<sub>65</sub>H<sub>82</sub>O<sub>10</sub>SSi

Synonyms:C₆₅H₈₂O₁₀SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₅H₈₂O₁₀SSi

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Technology Process of C₆₅H₈₂O₁₀SSi

There total 4 articles about C₆₅H₈₂O₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1294354-34-9
C₅₈H₇₆O₁₀SSi

: 100-39-0
benzyl bromide

: 1294354-35-0
C₆₅H₈₂O₁₀SSi

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/cbic.201000785

Reference yield:

: 2-O-acetyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranose trichloroacetimidate

: 1294354-35-0
C₆₅H₈₂O₁₀SSi

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 °C / Molecular sieve

2: methanol; sodium methylate / 20 °C

3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 20 °C

With methanol; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cbic.201000785

Reference yield:

: 1294354-24-7
C₃₂H₄₈O₇Si

: 1294354-35-0
C₆₅H₈₂O₁₀SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanethiol; mercury dibromide / acetonitrile / 20 °C

1.2: N-halosuccinimde / -20 °C

1.3: -20 °C

2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 °C / Molecular sieve

3.1: methanol; sodium methylate / 20 °C

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 20 °C

With methanol; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; ethanethiol; mercury dibromide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cbic.201000785