Technology Process of C13H10ClNO2S
There total 6 articles about C13H10ClNO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H9ClN2S;
With
sodium hydroxide;
In
ethanol;
at 80 ℃;
Large scale reaction;
With
hydrogenchloride; water;
Large scale reaction;
DOI:10.1021/op2003419
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bromine / methanol; acetonitrile / 0 - 5 °C / Large scale reaction
2.1: sodium sulfide / N,N-dimethyl-formamide / 0.5 h / 60 °C
2.2: 3 h / 60 °C
2.3: 60 °C
3.1: sodium hydroxide / ethanol / 80 °C / Large scale reaction
3.2: Large scale reaction
With
sodium sulfide; bromine; sodium hydroxide;
In
methanol; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/op2003419
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium sulfide / N,N-dimethyl-formamide / 0.5 h / 60 °C
1.2: 3 h / 60 °C
1.3: 60 °C
2.1: sodium hydroxide / ethanol / 80 °C / Large scale reaction
2.2: Large scale reaction
With
sodium sulfide; sodium hydroxide;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/op2003419