3,4-dimethoxyphenylpropioloyl chloride

Base Information

Chemical Name:3,4-dimethoxyphenylpropioloyl chloride
CAS No.:816462-34-7
Molecular Formula:C₁₁H₉ClO₃
Molecular Weight:224.644
Hs Code.:

Synonyms:3,4-dimethoxyphenylpropioloyl chloride

Suppliers and Price of 3,4-dimethoxyphenylpropioloyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-dimethoxyphenylpropioloyl chloride

Chemical Property:

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Technology Process of 3,4-dimethoxyphenylpropioloyl chloride

There total 5 articles about 3,4-dimethoxyphenylpropioloyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22511-06-4
3,4-dimethoxyphenylpropiolic acid

: 816462-34-7
3,4-dimethoxyphenylpropioloyl chloride

Guidance literature:: With thionyl chloride; In benzene; Heating;

Reference yield:

: 20583-78-2,24393-65-5
ethyl (E)-3,4-dimethoxycinnamate

: 816462-34-7
3,4-dimethoxyphenylpropioloyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: Br₂ / CH₂Cl₂ / 0 °C

2: KOH / ethanol / 4 h / Heating

3: SOCl₂ / CH₂Cl₂ / 3 h / Heating

With potassium hydroxide; thionyl chloride; bromine; In ethanol; dichloromethane;
DOI:10.1055/s-2001-18436

Reference yield:

: 14737-89-4
3,4-dimethoxy-trans-cinnamic acid

: 816462-34-7
3,4-dimethoxyphenylpropioloyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / 4 h / Heating

2: Br₂ / CH₂Cl₂ / 0 °C

3: KOH / ethanol / 4 h / Heating

4: SOCl₂ / CH₂Cl₂ / 3 h / Heating

With potassium hydroxide; thionyl chloride; bromine; In ethanol; dichloromethane;
DOI:10.1055/s-2001-18436