(1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

Base Information

Chemical Name:(1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate
CAS No.:1448344-52-2
Molecular Formula:C₂₃H₁₆Cl₂N₂O₆S
Molecular Weight:519.362
Hs Code.:

Synonyms:(1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

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Chemical Property of (1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

Chemical Property:

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Technology Process of (1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

There total 5 articles about (1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448345-05-8
C₁₆H₁₄N₂O₅S

: 89-75-8
2,4-dichlorobenzoyl chloride

: 1448344-52-2
(1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ol401666e

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1448344-52-2
(1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane / 0.5 h / 0 °C

1.2: 0.5 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

3.1: acetonitrile / 1 h / 20 °C

3.2: 4 h / 20 °C

4.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

With sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol401666e

Reference yield:

: 89241-33-8
1-(phenylsulfonyl)-3-(hydroxymethyl)indole

: 1448344-52-2
(1-(phenylsulfonyl)-1H-indol-3-yl)methyl 2,4-dichlorobenzoyloxycarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 1 h / 20 °C

1.2: 4 h / 20 °C

2.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

With triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol401666e