3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

Base Information

Chemical Name:3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester
CAS No.:857934-58-8
Molecular Formula:C₁₈H₂₈O₈
Molecular Weight:372.416
Hs Code.:

Synonyms:3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

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Chemical Property of 3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

Chemical Property:

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Technology Process of 3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

There total 2 articles about 3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 57722-04-0
1-chloro-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethane

: 857934-58-8
3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 24h;
DOI:10.1021/jo060217x

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 857934-58-8
3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine; thionyl chloride / CHCl₃ / 3 h / Heating

2: 91 percent / potassium carbonate; potassium iodide / dimethylformamide / 24 h / 60 °C

With pyridine; thionyl chloride; potassium carbonate; potassium iodide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo060217x

Reference yield:

: 857934-58-8
3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoic acid methyl ester

: 847342-67-0
2,2,2-trichloroacetimidic acid 3-methoxy-4-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / 0.75 h / 0 - 20 °C

2: 83 percent / sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo060217x