N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

Base Information

Chemical Name:N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate
CAS No.:1092467-10-1
Molecular Formula:C₄H₆O₆*C₂₅H₃₂N₂O₆
Molecular Weight:606.627
Hs Code.:

Synonyms:N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

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Chemical Property of N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

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Technology Process of N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

There total 5 articles about N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-69-4,138508-61-9
L-Tartaric acid

: 956895-37-7
N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide

: 1092467-10-1
N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

Guidance literature:: In water; isopropyl alcohol; at 50 - 56 ℃; for 0.333333h;

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1092467-10-1
N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

Guidance literature:: Multi-step reaction with 5 steps

1: N-benzyl-trimethylammonium hydroxide / methanol / 36 h / 78 °C / Inert atmosphere

2: hydrogenchloride; water / 3.5 h / 100 °C / Inert atmosphere

3: dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Inert atmosphere

4: dichloromethane / 2.5 h

5: water; isopropyl alcohol / 0.33 h / 50 - 56 °C

With hydrogenchloride; water; N-benzyl-trimethylammonium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 63815-39-4
2-(4-Methoxyphenoxy)cyanoethane

: 1092467-10-1
N-[2-hydroxy-2-(2,3-dihydrobenzo[β][1,4]dioxin-6-yl)-1-pyrrolidin-1-ylmethyl-ethyl]-3-(4-methoxy-phenoxy)-propionamide L-tartrate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / 3.5 h / 100 °C / Inert atmosphere

2: dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Inert atmosphere

3: dichloromethane / 2.5 h

4: water; isopropyl alcohol / 0.33 h / 50 - 56 °C

With hydrogenchloride; water; dicyclohexyl-carbodiimide; In dichloromethane; water; isopropyl alcohol;