tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

Base Information

Chemical Name:tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate
CAS No.:1443322-79-9
Molecular Formula:C₁₉H₂₄N₄O₅
Molecular Weight:388.423
Hs Code.:

Synonyms:tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

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Chemical Property of tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

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Technology Process of tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

There total 3 articles about tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256344-25-8
2-(2-nitrophenyl)propylamine

: C₁₀H₁₃ClN₂O₃

: 1443322-79-9
tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

Guidance literature:: With triethylamine; lithium chloride; In dichloromethane; at 0 - 20 ℃; for 20h;
DOI:10.1002/psc.2514

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1443322-79-9
tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C

2: triethylamine; dmap; 2-mesitylenesulphonyl chloride / dichloromethane / 6 h / 20 °C / Inert atmosphere

3: triethylamine; lithium chloride / dichloromethane / 20 h / 0 - 20 °C

With dmap; 2-mesitylenesulphonyl chloride; potassium carbonate; triethylamine; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/psc.2514

Reference yield:

: 257869-92-4
tert-butyl uracil-1-ylacetate

: 1443322-79-9
tert-butyl 2-(4-((2-(2-nitrophenyl)propyl)amino)-2-oxopyrimidin-1(2H)-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap; 2-mesitylenesulphonyl chloride / dichloromethane / 6 h / 20 °C / Inert atmosphere

2: triethylamine; lithium chloride / dichloromethane / 20 h / 0 - 20 °C

With dmap; 2-mesitylenesulphonyl chloride; triethylamine; lithium chloride; In dichloromethane;
DOI:10.1002/psc.2514