C₃₅H₂₆BrN

Base Information

• Chemical Name: C₃₅H₂₆BrN
• CAS No.: 1266612-86-5
• Molecular Formula: C₃₅H₂₆BrN
• Molecular Weight: 540.502
• Mol file: 1266612-86-5.mol

Synonyms:C₃₅H₂₆BrN

Chemical Property of C₃₅H₂₆BrN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₆BrN

There total 3 articles about C₃₅H₂₆BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

N-phenyl-(9,9-dimethyl-9H-fluoren-2-yl)amine (355832-04-1) + 1,8-dibromophenanthrene (20342-96-5) → C35H26BrN (1266612-86-5)

Guidance literature:

With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene; at 90 ℃; for 3h; Inert atmosphere;

Reference yield:

aniline (62-53-3) → C35H26BrN (1266612-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C / Inert atmosphere

2: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C / Inert atmosphere

With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene;

Reference yield:

2-bromo-9,9-dimethyl-9H-fluorene (28320-31-2) → C35H26BrN (1266612-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C / Inert atmosphere

2: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C / Inert atmosphere

With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene;

upstream raw materials:

aniline

2-bromo-9,9-dimethyl-9H-fluorene

N-phenyl-(9,9-dimethyl-9H-fluoren-2-yl)amine

1,8-dibromophenanthrene

Downstream raw materials:

C₄₈H₃₇N₃

C₄₉H₃₆N₂