1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Base Information

Chemical Name:1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene
CAS No.:1181844-99-4
Molecular Formula:C₄₆H₃₀O₂
Molecular Weight:614.743
Hs Code.:

Synonyms:1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

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Chemical Property of 1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

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Technology Process of 1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

There total 1 articles about 1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₆H₃₂Cl₂O₂

: 1181844-99-4
1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at -78 - -20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/anie.200901382

Reference yield: 99.0%

: 1181844-99-4
1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

: 1181845-00-0
1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Guidance literature:: With sodium tetrahydroborate; In ethanol; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.200901382