1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Base Information

• Chemical Name: 1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene
• CAS No.: 1181845-00-0
• Molecular Formula: C₄₆H₃₄O₂
• Molecular Weight: 618.775

Synonyms:1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Chemical Property of 1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Chemical Property:

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Technology Process of 1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

There total 1 articles about 1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene (1181844-99-4) → 1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene (1181845-00-0)

Guidance literature:

With sodium tetrahydroborate; In ethanol; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.200901382

Reference yield: 90.0%

1,2,3,9,10,11-hexahydro-1,9-/1,11-dihydroxy-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene (1181845-00-0) → 1,9-/1,11-dihydro-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene (1181845-01-1)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 90 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.200901382

upstream raw materials:

1,2,3,9,10,11-hexahydro-2-10-dimethyl-1,9-/-1,11-dioxo-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

Downstream raw materials:

1,9-/1,11-dihydro-2,10-dimethyl-6,14-diphenyl-s-indaceno[1,2,3-cd:5,6,7-c'd']diphenalene

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