N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide

Base Information

• Chemical Name: N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide
• CAS No.: 529488-41-3
• Molecular Formula: C₂₄H₂₇IN₄O₅
• Molecular Weight: 578.407

Synonyms:N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide

Chemical Property of N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide

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Technology Process of N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide

There total 8 articles about N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N'-(6,7-methylenedioxycinnolin-4-yl)-N,N-diethylethane-1,2-diamine + 2-iodo-4,5-dimethoxybenzoic acid (61203-48-3) → N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide (529488-41-3)

Guidance literature:

2-iodo-4,5-dimethoxybenzoic acid; With oxalyl dichloride; In dichloromethane; for 3h; Reflux;

N'-(6,7-methylenedioxycinnolin-4-yl)-N,N-diethylethane-1,2-diamine; With triethylamine; In dichloromethane; Reflux; Inert atmosphere;

Reference yield: 87.0%

2-iodo-4,5-dimethoxybenzoic acid (61203-48-3) + N'-(6,7-methylenedioxycinnolin-4-yl)-N,N-diethylethane-1,2-diamine (529485-94-7) → N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide (529488-41-3)

Guidance literature:

2-iodo-4,5-dimethoxybenzoic acid; With oxalyl dichloride; In dichloromethane; for 3h; Reflux;

N'-(6,7-methylenedioxycinnolin-4-yl)-N,N-diethylethane-1,2-diamine; With triethylamine; In dichloromethane; Reflux; Inert atmosphere;

Reference yield: 87.0%

4,5-dimethoxy-2-iodobenzoyl chloride (113258-92-7) + N'-(6,7-methylenedioxycinnolin-4-yl)-N,N-diethylethane-1,2-diamine (529485-94-7) → N-(6,7-methylenedioxycinnolin-4-yl)-N-[(2-N,N-diethylamino)ethyl]-2-iodo-4,5-dimethoxybenzamide (529488-41-3)

Guidance literature:

With triethylamine; In dichloromethane; for 16h; Heating;

DOI:10.1016/j.bmc.2003.10.061

upstream raw materials:

4,5-dimethoxy-2-iodobenzoyl chloride

N'-(6,7-methylenedioxycinnolin-4-yl)-N,N-diethylethane-1,2-diamine

2-iodo-4,5-dimethoxybenzoic acid

2-amino-4,5-methylenedioxy-acetophenone

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