C₂₆H₃₆Cl₄N₂W

Base Information

• Chemical Name: C₂₆H₃₆Cl₄N₂W
• CAS No.: 1430073-43-0
• Molecular Formula: C₂₆H₃₆Cl₄N₂W
• Molecular Weight: 702.247
• Mol file: 1430073-43-0.mol

Synonyms:C₂₆H₃₆Cl₄N₂W

Chemical Property of C₂₆H₃₆Cl₄N₂W

Chemical Property:

Purity/Quality:

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Technology Process of C₂₆H₃₆Cl₄N₂W

There total 2 articles about C₂₆H₃₆Cl₄N₂W which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

tungsten(VI) chloride (13283-01-7) + 1,2-bis(2,6-diisopropylphenylimino)ethane (74663-75-5,134750-23-5) → C26H36Cl4N2W (1430073-43-0)

Guidance literature:

tungsten(VI) chloride; With 1-methyl-3,6-bis(trimethylsilyl)-1,4-cyclohexadiene; In toluene; at -78 - 20 ℃; for 1h; Inert atmosphere;

1,2-bis(2,6-diisopropylphenylimino)ethane; In toluene; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ja401589a

Reference yield: 60.0%

tungsten(VI) chloride (13283-01-7) + 1,2-bis(2,6-diisopropylphenylimino)ethane (74663-75-5,134750-23-5) → C26H36Cl4N2W (1430073-43-0) + Cl6W(1-)*C23H29N2(1+)

Guidance literature:

In dichloromethane; at 20 ℃; for 18h;

DOI:10.1039/c7dt03226a

Reference yield: 70.0%

1,2-di(4-methylphenyl)-1,2-ethanedione (3457-48-5) + C26H36Cl4N2W (1430073-43-0) → C42H50Cl2N2O2W

Guidance literature:

With 1-methyl-3,6-bis(trimethylsilyl)-1,4-cyclohexadiene; In toluene; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ja401589a

upstream raw materials:

tungsten(VI) chloride

1,2-bis(2,6-diisopropylphenylimino)ethane