3,4-Bis-2-butenyl acetate

Base Information

Chemical Name:3,4-Bis-2-butenyl acetate
CAS No.:103223-43-4
Molecular Formula:C₂₂H₃₀O₂Si₂
Molecular Weight:382.65
Hs Code.:

3,4-Bis<dimethylphenylsilyl>-2-butenyl acetate

Synonyms:3,4-Bis-2-butenyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Bis-2-butenyl acetate

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Technology Process of 3,4-Bis-2-butenyl acetate

There total 2 articles about 3,4-Bis-2-butenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 103238-11-5
3,4-Bis-2-butenol

: 103223-43-4
3,4-Bis-2-butenyl acetate

Guidance literature:: With pyridine; at 80 ℃; for 4h;
DOI:10.1055/s-1985-31379

Reference yield:

: 3839-31-4
dimethyl(phenyl)silyllithium

: 103223-43-4
3,4-Bis-2-butenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) copper(I) cyanide / 1.) THF, 2.) 0 deg C, 1.5 h

2: 98 percent / pyridine / 4 h / 80 °C

With pyridine; copper(l) cyanide;
DOI:10.1055/s-1985-31379