methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Base Information

Chemical Name:methyl hexa-O-benzoyl-α-D-lactosuloside oxime
CAS No.:97523-58-5
Molecular Formula:C₅₅H₄₇NO₁₇
Molecular Weight:993.975
Hs Code.:

Synonyms:methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Suppliers and Price of methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl hexa-O-benzoyl-α-D-lactosuloside oxime

There total 7 articles about methyl hexa-O-benzoyl-α-D-lactosuloside oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 97523-59-6
methyl 3,6-di-O-benzoyl-2-(benzoyloximino)-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-arabino-hexopyranoside

: 97523-58-5
methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Guidance literature:: With hydrazine hydrate; In ethanol; water; for 2h; Ambient temperature;
DOI:10.1021/jo00219a017

Reference yield:

: 61198-91-2
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

: 97523-58-5
methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaI, 2.) diethylamine / 1.) acetone, RT, 15 min, 2.) RT, 16 h

2: 89 percent / hydroxylamine hydrochloride, pyridine / 20 h / 70 °C

3: 90 percent / pyridine / 4 h / Ambient temperature

4: 93 percent / N-bromosuccinimide / CCl₄ / 0.5 h / Heating; Irradiation

5: 62 percent / 3 h / Heating

With pyridine; N-Bromosuccinimide; hydroxylamine hydrochloride; diethylamine; sodium iodide; In tetrachloromethane;
DOI:10.1021/jo00219a017

Reference yield:

: 87760-36-9
2,3,6-tri-O-benzoyl-4-O-(2,3,4,5-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

: 97523-58-5
methyl hexa-O-benzoyl-α-D-lactosuloside oxime

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / hydroxylamine hydrochloride, pyridine / 20 h / 70 °C

2: 90 percent / pyridine / 4 h / Ambient temperature

3: 93 percent / N-bromosuccinimide / CCl₄ / 0.5 h / Heating; Irradiation

4: 62 percent / 3 h / Heating

With pyridine; N-Bromosuccinimide; hydroxylamine hydrochloride; In tetrachloromethane;
DOI:10.1021/jo00219a017