(S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride

Base Information

• Chemical Name: (S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride
• CAS No.: 848553-54-8
• Molecular Formula: C₃₁H₃₇N₇S*ClH
• Molecular Weight: 576.209

Synonyms:(S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride

Chemical Property of (S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride

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Technology Process of (S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride

There total 1 articles about (S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-5-[4-(2-methyl-4H-3-thia-9-azabenzo[f]azulen-10-yl)-2-phenethylpiperazin-1-yl]pentaneamide + dimethyltin oxide (2273-45-2) → (S)-2-methyl-10-[4-[4-(1-methyl-1H-tetrazol-5-yl)butyl]-3-phenethylpiperazin-1-yl]-4H-3-thia-9-azabenzo[f]azulene hydrochloride (848553-54-8)

Guidance literature:

(S)-5-[4-(2-methyl-4H-3-thia-9-azabenzo[f]azulen-10-yl)-2-phenethylpiperazin-1-yl]pentaneamide; dimethyltin oxide; With trimethylsilylazide; In toluene; at 20 ℃; for 18h; Heating / reflux;

With ammonia; In methanol; dichloromethane;

With hydrogenchloride; In diethyl ether; ethyl acetate;

upstream raw materials:

dimethyltin oxide

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