1-phenyl-3-methyl-2-butenyl propargyl ether

Base Information

Chemical Name:1-phenyl-3-methyl-2-butenyl propargyl ether
CAS No.:114709-69-2
Molecular Formula:C₁₄H₁₆O
Molecular Weight:200.28
Hs Code.:

Synonyms:1-phenyl-3-methyl-2-butenyl propargyl ether

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Chemical Property of 1-phenyl-3-methyl-2-butenyl propargyl ether

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Technology Process of 1-phenyl-3-methyl-2-butenyl propargyl ether

There total 1 articles about 1-phenyl-3-methyl-2-butenyl propargyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-86-8
3,3-dimethyl acrylaldehyde

: 591-51-5
phenyllithium

: 106-96-7
propargyl bromide

: 114709-69-2
1-phenyl-3-methyl-2-butenyl propargyl ether

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; Yield given. Multistep reaction; 1.) hexane, THF, 0 deg C, 15 min; 2.) 0 deg C, 15 min; 3.) 25 deg C, 3 h;
DOI:10.1246/bcsj.60.3465

Reference yield: 70.0%

: 892-20-6
triphenylstannane

: 114709-69-2
1-phenyl-3-methyl-2-butenyl propargyl ether

: (Z)-trans-3-isopropyl-2-phenyl-4-(triphenylstannylmethylene)oxolane

Guidance literature:: With triethyl borane; In hexane; toluene; under Ar, 1 M hexane soln. of Et3B added to soln. of Ph3SnH and enyne in toluene at 25°C, react. mixt. poured into water; extn. with ethyl acetate, preparative tlc; elem. anal.;
DOI:10.1246/bcsj.60.3465

Reference yield:

: 114709-69-2
1-phenyl-3-methyl-2-butenyl propargyl ether

: (2R,3R)-3-Isopropyl-4-methylene-2-phenyl-tetrahydro-furan

Guidance literature:: With n-butyllithium; triethyl borane; triphenylstannane; Yield given. Multistep reaction; 1.) hexane, toluene, 25 deg C, 3 h; 2.) hexane, THF, -78 deg C, 15 min,;
DOI:10.1246/bcsj.60.3465