3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

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Chemical Name:3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile
CAS No.:1287784-28-4
Molecular Formula:C₂₈H₃₂N₂O₂S₁₀
Molecular Weight:749.234
Hs Code.:

Synonyms:3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

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Chemical Property of 3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

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Technology Process of 3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

There total 1 articles about 3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 132765-35-6
4,5-bis((2-cyanoethyl)thio)-1,3-dithiole-2-thione

: 295806-73-4
1,4-bis(bromomethyl)-2,5-dibutyloxybenzene

: 1287784-28-4
3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

Guidance literature:: 4,5-bis((2-cyanoethyl)thio)-1,3-dithiole-2-thione; With cesiumhydroxide monohydrate; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 1.25h; Inert atmosphere;

1,4-bis(bromomethyl)-2,5-dibutyloxybenzene; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 4.5h; Inert atmosphere;
DOI:10.1055/s-0030-1258297

Reference yield: 72.0%

: 1287784-27-3
3-[(5-{[4-(bromomethyl)-2,5-dibutoxybenzyl]sulfanyl}-2-thioxo-1,3-dithiol-4-yl)sulfanyl]propanenitrile

: 1287784-28-4
3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

: 1287784-29-5
3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2,5-dibutoxybenzene-4,1-diyl)methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile

Guidance literature:: 3,3'-{(2,5-dibutoxybenzene-1,4-diyl)bis[methanediylsulfanediyl(2-thioxo-1,3-dithiole-5,4-diyl)sulfanediyl]}dipropanenitrile; With cesiumhydroxide monohydrate; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 1.25h; Inert atmosphere;

3-[(5-{[4-(bromomethyl)-2,5-dibutoxybenzyl]sulfanyl}-2-thioxo-1,3-dithiol-4-yl)sulfanyl]propanenitrile; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 4.5h; Inert atmosphere;
DOI:10.1055/s-0030-1258297