4-cinnamylbenzonitrile

Base Information

Chemical Name:4-cinnamylbenzonitrile
CAS No.:1119892-52-2
Molecular Formula:C₁₆H₁₃N
Molecular Weight:219.286
Hs Code.:

Synonyms:4-cinnamylbenzonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-cinnamylbenzonitrile

Chemical Property:

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Technology Process of 4-cinnamylbenzonitrile

There total 4 articles about 4-cinnamylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 104-54-1
3-Phenylpropenol

: 126747-14-6
4-cyanophenylboronic acid

: 1119892-52-2
4-cinnamylbenzonitrile

Guidance literature:: With potassium phosphate; C₄₅H₄₅N₉Ni⁽²⁺⁾*2CF₃O₃S^(1-); zinc; In benzene; at 80 ℃; for 16h; Reagent/catalyst; Inert atmosphere;
DOI:10.1002/adsc.202000186

Reference yield:

: C₁₆H₁₂BrN

: 1119892-52-2
4-cinnamylbenzonitrile

: C₁₆H₁₃N

Guidance literature:: With iron(III) chloride hexahydrate; benzyl alcohol; In toluene; at 80 ℃; for 4h; Overall yield = 62 %;
DOI:10.1007/s11426-013-5042-2

Reference yield:

: 591-50-4
iodobenzene

: 1119892-52-2
4-cinnamylbenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; silver carbonate / toluene / 12 h / Reflux; Schlenk technique

2: palladium diacetate; potassium fluoride / methanol / 12 h / 70 °C / Schlenk technique

With potassium fluoride; palladium diacetate; silver carbonate; In methanol; toluene;
DOI:10.1002/anie.201705671