carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

Base Information

Chemical Name:carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O
CAS No.:934672-37-4
Molecular Formula:C₂₉H₃₅O₂PRu
Molecular Weight:547.639
Hs Code.:

Synonyms:carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

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Chemical Property of carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

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Technology Process of carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

There total 1 articles about carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)(O)dicarbonylruthenium(II) (PF6) - dichloromethane (1/1)

: 934672-37-4
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

Guidance literature:: With (CH₃)3NO*2H₂O; In methanol; (Ar), Ru complex and (CH3)3NO*2H2O stirred overnight; dissolved (hot CH2Cl2), concd. (Ar stream), crystd. at -20°C, elem. anal.;
DOI:10.1002/ejic.200501051

Reference yield: 96.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 934672-37-4
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

: 918134-45-9
chlorocarbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2CO(t-Bu)O

Guidance literature:: In methanol; water; (Ar), aq.HCl added to a slurry of Ru complex in cold (-80°C) CH3OH, warmed to room temp., stirred for 1 h; evapd.(vac.), extd.(Et2O), filtered, evapd.(vac.), elem. anal.;
DOI:10.1002/ejic.200501051

Reference yield: 88.0%

: 934672-37-4
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

: 67969-83-9
tetrafluoroboric acid dimethyl ether complex

: 918134-54-0
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (BF4)

Guidance literature:: In methanol; (Ar), HBF4*OMe2 in CH3OH added to Ru complex in cold (-80°C) CH3OH, warmed to room temp., stirred for 1 h; evapd.(vac.), dissolved (CH2Cl2), crystd.(CH3OH/Et2O), elem. anal.;
DOI:10.1002/ejic.200501051