carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

Base Information

Chemical Name:carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)
CAS No.:918134-44-8
Molecular Formula:C₂₉H₃₆O₂PRu*F₆P
Molecular Weight:693.612
Hs Code.:

Synonyms:carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

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Chemical Property of carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

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Technology Process of carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

There total 1 articles about carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: hexafluorophosphoric acid

: 934672-37-4
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCHC(t-Bu)O

: 918134-44-8
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

Guidance literature:: In methanol; water; (Ar), aq.HPF6 added to Ru complex in cold (-80°C) CH3OH, warmed to room temp., stirred for 1 h; evapd.(vac.), dissolved (CH2Cl2), crystd.(CH3OH/Et2O), elem. anal.;
DOI:10.1002/ejic.200501051

Reference yield: 88.0%

: 918134-44-8
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

: 3923-52-2
1,1-diphenyl-2-propyn-1-ol

: carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O)(MeOCCHCPh2) (PF6)

Guidance literature:: In methanol; (Ar), Ru complex and ligand in CH3OH stirred at room temp. for 20 h; pptd., filtered, washed (Et2O), dissolved (CH2Cl2), crystd.(CH3OH/Et2O),elem. anal.;
DOI:10.1002/ejic.200501051

Reference yield: 88.0%

: 918134-44-8
carbonylruthenium(II)(η5-pentamethylcyclopentadienyl)(Ph2PCH2C(t-Bu)O (PF6)

: 74-86-2,25067-58-7
acetylene

: [Ru(C(Me)OMe)(η5-C5Me5)(Ph2PCH2CP(tBu))(CO)]PF6

Guidance literature:: In methanol; soln. of Ru complex in CH3OH stirred at room temp. under atm. of ethyne for 24 h; evapn. under vac., residue dissolved in CH2Cl2, soln. layered with Et2O,crystals isolated; elem. anal.;
DOI:10.1002/ejic.200900574