C₂₅H₂₅BrO₇S₂

Base Information

Chemical Name:C₂₅H₂₅BrO₇S₂
CAS No.:307492-90-6
Molecular Formula:C₂₅H₂₅BrO₇S₂
Molecular Weight:581.505
Hs Code.:

C<sub>25</sub>H<sub>25</sub>BrO<sub>7</sub>S<sub>2</sub>

Synonyms:C₂₅H₂₅BrO₇S₂

Suppliers and Price of C₂₅H₂₅BrO₇S₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₅BrO₇S₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₅BrO₇S₂

There total 11 articles about C₂₅H₂₅BrO₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 307492-86-0
C₂₅H₂₆O₇S₂

: 307492-90-6
C₂₅H₂₅BrO₇S₂

Guidance literature:: With N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide; In tetrachloromethane; for 9h; Heating;
DOI:10.1002/1099-0690(200009)2000:18<3223::AID-EJOC3223>3.0.CO;2-L

Reference yield:

: 25458-46-2
4-methoxyphenyl methoxymethyl ether

: 307492-90-6
C₂₅H₂₅BrO₇S₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: nBuLi / tetrahydrofuran; hexane; diethyl ether / 6 h / 25 °C

1.2: 85 percent / CuI / tetrahydrofuran; hexane; diethyl ether / -78 °C

2.1: SeO₂ / ethanol / 0.5 h / Heating

2.2: 80 percent / NaBH₄ / ethanol / 1 h / 0 °C

3.1: 88 percent / Ti(OiPr)4; D-(-)-diethyl tartrate; tBuOOH / CH₂Cl₂; toluene / 24 h / -24 °C

4.1: 95 percent / LiAlH₄ / diethyl ether / 5 h / 25 °C

5.1: 95 percent / TsOH / 0.5 h / 25 °C

6.1: ammonium ceric nitrate / acetonitrile; H₂O / 2 h / -5 °C

6.2: 1 mol/l HCl / methanol; H₂O / 24 h / 25 °C

7.1: 80 percent / Red-Al / tetrahydrofuran / 1.5 h / 0 °C

8.1: 81 percent / Et₃N; 4-dimethylaminopyridine / 4 h / 0 - 20 °C

9.1: 80 percent / N-bromosuccinimide; K₂CO₃; dibenzoyl peroxide / CCl₄ / 9 h / Heating

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; selenium(IV) oxide; ammonium cerium(IV) nitrate; diethyl (2S,3S)-tartrate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; diethyl ether; ethanol; hexane; dichloromethane; water; toluene; acetonitrile; 1.1: Metallation / 2.1: Oxidation / 3.1: Sharpless epoxidation / 4.1: Reduction / 5.1: Cyclization / 6.1: Oxidation / 6.2: cyclization / 7.1: Reduction / 8.1: Tosylation / 9.1: Bromination;
DOI:10.1002/1099-0690(200009)2000:18<3223::AID-EJOC3223>3.0.CO;2-L

Reference yield:

: 150-76-5
4-methoxy-phenol

: 307492-90-6
C₂₅H₂₅BrO₇S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: 97 percent / iPr₂NEt / CH₂Cl₂ / 12 h / 40 °C

2.1: nBuLi / tetrahydrofuran; hexane; diethyl ether / 6 h / 25 °C

2.2: 85 percent / CuI / tetrahydrofuran; hexane; diethyl ether / -78 °C

3.1: SeO₂ / ethanol / 0.5 h / Heating

3.2: 80 percent / NaBH₄ / ethanol / 1 h / 0 °C

4.1: 88 percent / Ti(OiPr)4; D-(-)-diethyl tartrate; tBuOOH / CH₂Cl₂; toluene / 24 h / -24 °C

5.1: 95 percent / LiAlH₄ / diethyl ether / 5 h / 25 °C

6.1: 95 percent / TsOH / 0.5 h / 25 °C

7.1: ammonium ceric nitrate / acetonitrile; H₂O / 2 h / -5 °C

7.2: 1 mol/l HCl / methanol; H₂O / 24 h / 25 °C

8.1: 80 percent / Red-Al / tetrahydrofuran / 1.5 h / 0 °C

9.1: 81 percent / Et₃N; 4-dimethylaminopyridine / 4 h / 0 - 20 °C

10.1: 80 percent / N-bromosuccinimide; K₂CO₃; dibenzoyl peroxide / CCl₄ / 9 h / Heating

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; selenium(IV) oxide; ammonium cerium(IV) nitrate; diethyl (2S,3S)-tartrate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; diethyl ether; ethanol; hexane; dichloromethane; water; toluene; acetonitrile; 1.1: Alkylation / 2.1: Metallation / 3.1: Oxidation / 4.1: Sharpless epoxidation / 5.1: Reduction / 6.1: Cyclization / 7.1: Oxidation / 7.2: cyclization / 8.1: Reduction / 9.1: Tosylation / 10.1: Bromination;
DOI:10.1002/1099-0690(200009)2000:18<3223::AID-EJOC3223>3.0.CO;2-L