3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

Base Information

Chemical Name:3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile
CAS No.:126921-96-8
Molecular Formula:C₁₅H₁₂N₂O
Molecular Weight:236.273
Hs Code.:
Mol file:126921-96-8.mol

Synonyms:3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

Suppliers and Price of 3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

Chemical Property:

Melting Point:>300 °C
Boiling Point:546.3±50.0 °C(Predicted)
PKA:9.74±0.60(Predicted)
Density:1.27±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

There total 5 articles about 3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 5407-83-0
ethyl 2-cyano-2-cyclopentylideneacetate

: 100-52-7
benzaldehyde

: 126921-96-8
3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

Guidance literature:: With ammonium acetate; for 5h; Heating;

Reference yield:

: 106961-65-3
(2-Morpholin-4-yl-cyclopent-1-enyl)-phenyl-methanone

: 107-91-5
cyanoacetic acid amide

: 126921-96-8
3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

Guidance literature:: With diethylamine; In benzene; for 10h; Reflux;
DOI:10.1134/S1070428021100250

Reference yield:

: 120-92-3
cyclopentanone

: 126921-96-8
3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / benzene / 5 h / Reflux

2: triethylamine / benzene / 6 h / 35 - 40 °C

3: diethylamine / benzene / 10 h / Reflux

With toluene-4-sulfonic acid; diethylamine; triethylamine; In benzene;
DOI:10.1134/S1070428021100250