N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

Base Information

Chemical Name:N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide
CAS No.:1053223-46-3
Molecular Formula:C₂₅H₃₉ClNOP
Molecular Weight:436.018
Hs Code.:

Synonyms:N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

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Technology Process of N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

There total 1 articles about N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 79606-45-4
N,N-diisopropyl 4-chlorobenzamide

: 16523-54-9
chlorodicyclohexylphosphane

: 1053223-46-3
N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

Guidance literature:: N,N-diisopropyl 4-chlorobenzamide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.583333h; Inert atmosphere;

chlorodicyclohexylphosphane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200800318

Reference yield: 87.0%

: 4426-47-5
butylboronic acid

: 1053223-46-3
N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

: 1053223-50-9
N,N-diisopropyl 4-n-butyl-2-dicyclohexylphosphinobenzamide

Guidance literature:: With potassium phosphate; palladium diacetate; In tetrahydrofuran; at 80 ℃; for 8h; Inert atmosphere;
DOI:10.1002/chem.200800318

Reference yield: 87.0%

: 1053223-46-3
N,N-diisopropyl 4-chloro-2-dicyclohexylphosphinobenzamide

: 98-80-6
phenylboronic acid

: 680218-52-4
N,N-diisopropyl 2-dicyclohexylphosphino-4-phenylbenzamide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride dihydrate; In toluene; at 20 - 110 ℃;
DOI:10.1002/chem.200800318