C₃₁H₃₈N₂O₆Si

Base Information

Chemical Name:C₃₁H₃₈N₂O₆Si
CAS No.:946407-87-0
Molecular Formula:C₃₁H₃₈N₂O₆Si
Molecular Weight:562.738
Hs Code.:

C<sub>31</sub>H<sub>38</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₁H₃₈N₂O₆Si

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Chemical Property of C₃₁H₃₈N₂O₆Si

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Technology Process of C₃₁H₃₈N₂O₆Si

There total 8 articles about C₃₁H₃₈N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₄₀O₆Si

: 946407-87-0
C₃₁H₃₈N₂O₆Si

Guidance literature:: With 4-toluenesulfonyl azide; TEA; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2007.05.041

Reference yield:

: 185385-63-1
C₁₃H₁₈O₄

: 946407-87-0
C₃₁H₃₈N₂O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: LiAlH₄ / diethyl ether / 0.33 h / 0 °C

2: imidazole / CH₂Cl₂; dimethylformamide / 24 h / 20 °C

3: (DHQD)2PHAL; K₃Fe(CN)6; K₂CO₃ / K₂OsO₂(OH)4 / 2-methyl-propan-2-ol; H₂O / 12 h / 20 °C

4: NaIO₄ / methanol; H₂O / 1 h / 20 °C

5: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 36 h / 20 °C

6: tetrahydrofuran / 1 h

7: tetrahydrofuran / 41 h

8: TsN₃; TEA / acetonitrile / 4 h / 20 °C

With 1H-imidazole; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; lithium aluminium tetrahydride; 4-toluenesulfonyl azide; 2-methyl-but-2-ene; TEA; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); potassium dioxotetrahydroxoosmate(VI); In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 3: Sharpless dihydroxylation;
DOI:10.1016/j.tetlet.2007.05.041

Reference yield:

: C₁₂H₁₈O₃

: 946407-87-0
C₃₁H₃₈N₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: imidazole / CH₂Cl₂; dimethylformamide / 24 h / 20 °C

2: (DHQD)2PHAL; K₃Fe(CN)6; K₂CO₃ / K₂OsO₂(OH)4 / 2-methyl-propan-2-ol; H₂O / 12 h / 20 °C

3: NaIO₄ / methanol; H₂O / 1 h / 20 °C

4: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 36 h / 20 °C

5: tetrahydrofuran / 1 h

6: tetrahydrofuran / 41 h

7: TsN₃; TEA / acetonitrile / 4 h / 20 °C

With 1H-imidazole; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 4-toluenesulfonyl azide; 2-methyl-but-2-ene; TEA; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); potassium dioxotetrahydroxoosmate(VI); In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 2: Sharpless dihydroxylation;
DOI:10.1016/j.tetlet.2007.05.041