2,3-bis-benzyloxy-5-iodo-terephthalic acid

Base Information

Chemical Name:2,3-bis-benzyloxy-5-iodo-terephthalic acid
CAS No.:350245-30-6
Molecular Formula:C₂₂H₁₇IO₆
Molecular Weight:504.278
Hs Code.:

Synonyms:2,3-bis-benzyloxy-5-iodo-terephthalic acid

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Chemical Property of 2,3-bis-benzyloxy-5-iodo-terephthalic acid

Chemical Property:

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Technology Process of 2,3-bis-benzyloxy-5-iodo-terephthalic acid

There total 8 articles about 2,3-bis-benzyloxy-5-iodo-terephthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 350245-27-1
2,3-bis-benzyloxy-5-iodo-terephthalic acid dimethyl ester

: 350245-30-6
2,3-bis-benzyloxy-5-iodo-terephthalic acid

Guidance literature:: 2,3-bis-benzyloxy-5-iodo-terephthalic acid dimethyl ester; With lithium hydroxide; In tetrahydrofuran; water;

With potassium hydroxide; In methanol; water; Heating;
DOI:10.1016/S0040-4039(01)00524-X

Reference yield:

: 7168-94-7
dimethyl 2,3-dimethoxyterephthalate

: 350245-30-6
2,3-bis-benzyloxy-5-iodo-terephthalic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: AgNO₃; TFAA

2.1: H₂ / Raney Ni

3.1: H(+); NaNO₂; KI

4.1: BBr₃

4.2: 86 percent / K₂CO₃

5.1: LiOH / H₂O; tetrahydrofuran

5.2: 100 percent / KOH / H₂O; methanol / Heating

With lithium hydroxide; hydrogen; hydrogen cation; boron tribromide; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite; nickel; In tetrahydrofuran; water; 1.1: Crivello method / 3.1: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X

Reference yield:

: 75956-62-6
dimethyl 2,3-dihydroxyterephthalate

: 350245-30-6
2,3-bis-benzyloxy-5-iodo-terephthalic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / K₂CO₃

2.1: AgNO₃; TFAA

3.1: H₂ / Raney Ni

4.1: H(+); NaNO₂; KI

5.1: BBr₃

5.2: 86 percent / K₂CO₃

6.1: LiOH / H₂O; tetrahydrofuran

6.2: 100 percent / KOH / H₂O; methanol / Heating

With lithium hydroxide; hydrogen; hydrogen cation; boron tribromide; potassium carbonate; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite; nickel; In tetrahydrofuran; water; 2.1: Crivello method / 4.1: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X