di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

Base Information

Chemical Name:di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate
CAS No.:229486-32-2
Molecular Formula:C₂₈H₄₅N₅O₈
Molecular Weight:579.694
Hs Code.:

Synonyms:di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

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Chemical Property of di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

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Technology Process of di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

There total 7 articles about di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 4530-20-5
BOC-glycine

: 229486-31-1
N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

: 229486-32-2
di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; at 0 ℃;

Reference yield: 77.0%

: 56406-63-4
N-(tert-butoxycarbonyl)glycine succinimide ester

: 229486-31-1
N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

: 229486-32-2
di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

Guidance literature:: In 1,4-dioxane; chloroform; at 20 ℃; for 0.75h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 229486-32-2
di-tert-butyl 3-(4-benzyloxycarbonylaminobutyl)-4,9-dioxo-2,5,8,11-tetraazadodecanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / CH₂Cl₂; CHCl₃

2: 89 percent / methanol / 20 °C

3: 96 percent / DCC / dioxane / 0 °C

With triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; dichloromethane; chloroform; 1: Condensation / 2: Substitution / 3: Condensation;