2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

Base Information

Chemical Name:2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid
CAS No.:1160707-77-6
Molecular Formula:C₁₂H₁₈BNO₅
Molecular Weight:267.09
Hs Code.:

Synonyms:2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

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Chemical Property of 2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

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Technology Process of 2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

There total 2 articles about 2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 85630-19-9
N,N-diethyl-1-carbamyloxy-2-methoxybenzene

: 7732-18-5
water

: 1160707-77-6
2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

Guidance literature:: With CH₃CH(Li)CH₂CH₃; (CH₃)2NCH₂CH₂N(CH₃)2; In tetrahydrofuran; treatment of sulfam deriv. with sec-butyllithium and TMEDA in THF at -78°C, treatment with trimethylborate and then with water;
DOI:10.1021/ja200398c

Reference yield:

: C₁₄H₂₂BNO₅

: 1160707-77-6
2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; pH=5 - 6;
DOI:10.1021/jo900146d

Reference yield: 91.0%

: 1160707-77-6
2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid

: 76881-19-1
5,5-dimethyl-3-trifluoromethylsulfonyloxycyclohex-2-en-1-one

: N,N-diethyl 2-(5',5'-dimethyl-3'-oxocyclohexenyl)-6-methoxyphenyl carbamate

Guidance literature:: 5,5-dimethyl-3-trifluoromethylsulfonyloxycyclohex-2-en-1-one; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; at 20 ℃; for 0.166667h;

2-(N,N-diethylcarbamoyloxy)-3-methoxyphenylboronic acid; With sodium carbonate; In 1,2-dimethoxyethane; ethanol; water; for 18h; Reflux;
DOI:10.1055/s-0037-1610273