C₂₂H₁₆F₃NO₃

Base Information

Chemical Name:C₂₂H₁₆F₃NO₃
CAS No.:1367127-50-1
Molecular Formula:C₂₂H₁₆F₃NO₃
Molecular Weight:399.369
Hs Code.:

C<sub>22</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>3</sub>

Synonyms:C₂₂H₁₆F₃NO₃

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Chemical Property of C₂₂H₁₆F₃NO₃

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Technology Process of C₂₂H₁₆F₃NO₃

There total 4 articles about C₂₂H₁₆F₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1367127-48-7
C₂₀H₁₃ClF₃NO₃

: 75927-49-0
pinacol vinylboronate

: 1367127-50-1
C₂₂H₁₆F₃NO₃

Guidance literature:: With tetrabutyl ammonium fluoride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; for 3h; Inert atmosphere; Heating;

Reference yield:

: 88912-25-8
4,6-dichloro-2-pyridinecarboxylic acid

: 1367127-50-1
C₂₂H₁₆F₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; ethanol; water / 3.5 h / 60 °C / Inert atmosphere

1.2: 20 °C / pH 1

2.1: hydrogenchloride / 1,4-dioxane / 12 h / 20 °C

3.1: tetrabutyl ammonium fluoride / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / tetrahydrofuran / 3 h / Inert atmosphere; Heating

With hydrogenchloride; tetrabutyl ammonium fluoride; caesium carbonate; bis-triphenylphosphine-palladium(II) chloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; ethanol; water;

Reference yield:

: 1367127-40-9
4,4,5,5-tetramethyl-2-(4-(4-(trifluoromethyl)phenoxy)phenyl)-1,3,2-dioxaborolane

: 1367127-50-1
C₂₂H₁₆F₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; ethanol; water / 3.5 h / 60 °C / Inert atmosphere

1.2: 20 °C / pH 1

2.1: hydrogenchloride / 1,4-dioxane / 12 h / 20 °C

3.1: tetrabutyl ammonium fluoride / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / tetrahydrofuran / 3 h / Inert atmosphere; Heating

With hydrogenchloride; tetrabutyl ammonium fluoride; caesium carbonate; bis-triphenylphosphine-palladium(II) chloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; ethanol; water;