ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

Base Information

Chemical Name:ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal
CAS No.:93184-26-0
Molecular Formula:C₂₁H₂₁Cl₂NO₇
Molecular Weight:470.306
Hs Code.:

Synonyms:ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

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Technology Process of ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

There total 5 articles about ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 105-36-2
ethyl bromoacetate

: 93135-35-4
2,3-dichloro-4-<(4-nitrophenyl)acetyl>phenol 1,2-propylene ketal

: 93184-26-0
ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

Guidance literature:: With potassium carbonate; In butanone; for 2h; Heating;
DOI:10.1021/jm00379a016

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 93184-26-0
ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / AlCl₃ / CH₂Cl₂ / 2 h / Heating

2: 66 percent / 48percent HBr / acetic acid / 22 h / Heating

3: 89 percent / p-TsOH / toluene / 19 h / Heating

4: 86 percent / K₂CO₃ / butan-2-one / 2 h / Heating

With aluminium trichloride; hydrogen bromide; potassium carbonate; toluene-4-sulfonic acid; In dichloromethane; acetic acid; toluene; butanone;
DOI:10.1021/jm00379a016

Reference yield:

: 93184-25-9
2,3-dichloro-4-<(4-nitrophenyl)acetyl>phenol

: 93184-26-0
ethyl <2,3-sdichloro-4-<(4-nitrophenyl)acetyl>phenoxy>acetate 1,2-propylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / p-TsOH / toluene / 19 h / Heating

2: 86 percent / K₂CO₃ / butan-2-one / 2 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; In toluene; butanone;
DOI:10.1021/jm00379a016