(2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Base Information

Chemical Name:(2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene
CAS No.:172281-53-7
Molecular Formula:C₅₄H₈₅NO₉
Molecular Weight:892.27
Hs Code.:

Synonyms:(2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Suppliers and Price of (2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

There total 7 articles about (2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103348-50-1
(2S,3R,4E)-2-azido-3-benzoyloxy-4-octadecen-1-ol

: 172281-53-7
(2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / SnCl₄, 4 Angstroem molecular sieves / CH₂Cl₂; hexane / 1 h

2: 89 percent / NaOMe / CH₂Cl₂; methanol / 3 h / -70 - -50 °C

3: 45 percent / HCOOH / 0.75 h / 22 °C

4: H₂S, pyridine / H₂O / 18 h / 22 °C

5: NaOAc, water / tetrahydrofuran

With pyridine; formic acid; 4 A molecular sieve; hydrogen sulfide; water; sodium methylate; sodium acetate; tin(IV) chloride; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/jm9606960

Reference yield:

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: 172281-53-7
(2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / SnCl₄, 4 Angstroem molecular sieves / CH₂Cl₂; hexane / 1 h

2: 89 percent / NaOMe / CH₂Cl₂; methanol / 3 h / -70 - -50 °C

3: 45 percent / HCOOH / 0.75 h / 22 °C

4: H₂S, pyridine / H₂O / 18 h / 22 °C

5: NaOAc, water / tetrahydrofuran

With pyridine; formic acid; 4 A molecular sieve; hydrogen sulfide; water; sodium methylate; sodium acetate; tin(IV) chloride; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/jm9606960

Reference yield:

: 100-52-7
benzaldehyde

: 172281-53-7
(2S,3R,4E)-3-(benzoyloxy)-2-(hexadecanoylamino)-1-[(4,6-O-benzylidene-β-D-galactopyranosyl)oxy]-4-octadecene

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / HCOOH / 0.75 h / 22 °C

2: H₂S, pyridine / H₂O / 18 h / 22 °C

3: NaOAc, water / tetrahydrofuran

With pyridine; formic acid; hydrogen sulfide; water; sodium acetate; In tetrahydrofuran; water;
DOI:10.1021/jm9606960