N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide
CAS No.:1382240-46-1
Molecular Formula:C₂₈H₂₅NO₃S
Molecular Weight:455.577
Hs Code.:

Synonyms:N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

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Chemical Property of N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

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Technology Process of N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

There total 4 articles about N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 857026-45-0
N-allyl-N-(3-(2-formylphenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

: 536-74-3
phenylacetylene

: 1382240-46-1
N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

N-allyl-N-(3-(2-formylphenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1039/c9cc08286g

Reference yield:

: 26260-02-6
2-iodobenzaldehyde

: 1382240-46-1
N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / Inert atmosphere

2: tetrahydrofuran / 6 h / 70 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran;
DOI:10.1021/ol301322a

Reference yield:

: 133886-40-5
N-tosyl-N-allylpropargylamine

: 1382240-46-1
N-allyl-N-(3-(2-(1-hydroxy-3-phenylprop-2-yn-1-yl)phenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / Inert atmosphere

2: tetrahydrofuran / 6 h / 70 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran;
DOI:10.1021/ol301322a