4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

Base Information

Chemical Name:4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol
CAS No.:1284150-03-3
Molecular Formula:C₂₄H₂₁ClN₂O₃
Molecular Weight:420.895
Hs Code.:

Synonyms:4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

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Chemical Property of 4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

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Technology Process of 4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

There total 3 articles about 4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13031-43-1
4-acetyloxyacetophenone

: 1284150-03-3
4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium hydrobromide perbromide / 1,4-dioxane / 5 h

2.1: sodium hydrogencarbonate / methanol; dichloromethane

3.1: tetrahydrofuran / 0.08 h / -78 °C

3.2: 1 h / Cooling

4.1: ammonium acetate / acetic acid / 100 - 110 °C

With pyridinium hydrobromide perbromide; ammonium acetate; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetic acid;

Reference yield:

: 41104-10-3
acetic acid 4-(2-bromoacetyl)phenyl ester

: 1284150-03-3
4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / methanol; dichloromethane

2.1: tetrahydrofuran / 0.08 h / -78 °C

2.2: 1 h / Cooling

3.1: ammonium acetate / acetic acid / 100 - 110 °C

With ammonium acetate; sodium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; acetic acid;

Reference yield:

: 1067425-94-8
acetic acid 4-{2-[4-(4-chloro-phenoxy)-phenylamino]-acetyl}-phenyl ester

: 1284150-03-3
4-{1-[4-(4-chloro-phenoxy)-phenyl]-2-ethoxymethyl-1H-imidazol-4-yl}-phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 0.08 h / -78 °C

1.2: 1 h / Cooling

2.1: ammonium acetate / acetic acid / 100 - 110 °C

With ammonium acetate; In tetrahydrofuran; acetic acid;