C₃₃H₄₃FN₆O₅

Base Information

Chemical Name:C₃₃H₄₃FN₆O₅
CAS No.:1009092-11-8
Molecular Formula:C₃₃H₄₃FN₆O₅
Molecular Weight:622.74
Hs Code.:

C<sub>33</sub>H<sub>43</sub>FN<sub>6</sub>O<sub>5</sub>

Synonyms:C₃₃H₄₃FN₆O₅

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Chemical Property of C₃₃H₄₃FN₆O₅

Chemical Property:

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Technology Process of C₃₃H₄₃FN₆O₅

There total 9 articles about C₃₃H₄₃FN₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1009092-10-7
C₁₅H₂₂BNO₄

: 1009092-09-4
C₂₄H₃₃BrFN₅O₃

: 1009092-11-8
C₃₃H₄₃FN₆O₅

Guidance literature:: With potassium acetate; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; at 60 ℃; for 2h;

Reference yield:

: 149947-15-9
3-bromo-2-fluorobenzaldehyde

: 1009092-11-8
C₃₃H₄₃FN₆O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9

2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

2.2: pH 7

3.1: calcium chloride / diethyl ether / 3 h / 20 °C

4.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation

4.2: 2 h

5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

6.2: 2 h

6.3: 5 h

7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 60 °C

With titanium(IV) isopropylate; hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; calcium chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; water; dimethyl sulfoxide; toluene;

Reference yield:

: 304876-62-8
C₇H₅BrFNO

: 1009092-11-8
C₃₃H₄₃FN₆O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

1.2: pH 7

2.1: calcium chloride / diethyl ether / 3 h / 20 °C

3.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation

3.2: 2 h

4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

5.2: 2 h

5.3: 5 h

6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 60 °C

With titanium(IV) isopropylate; hydrogenchloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; calcium chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; water; dimethyl sulfoxide; toluene;