3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

Base Information

Chemical Name:3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one
CAS No.:140860-63-5
Molecular Formula:C₁₉H₁₈O₅
Molecular Weight:326.349
Hs Code.:

Synonyms:3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

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Chemical Property of 3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

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Technology Process of 3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

There total 3 articles about 3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 140860-61-3
(4R,5S)-5-Benzo[1,3]dioxol-5-yl-4-hydroxymethyl-3-[1-phenyl-meth-(E)-ylidene]-dihydro-furan-2-one

: 140860-63-5
3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;

Reference yield:

: 16108-37-5,105602-23-1,139219-16-2,139219-49-1
trans-4-hydroxymethyl-5-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

: 140860-63-5
3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium methoxide, 2.) dil. sulfuric acid / 1.) benzene 2.) 4 h

2: 98 percent / H₂ / 10 percent Pd-C / ethyl acetate

With sulfuric acid; hydrogen; sodium methylate; palladium on activated charcoal; In ethyl acetate;

Reference yield:

: 100-52-7
benzaldehyde

: 140860-63-5
3α-benzyl-4β-hydroxymethyl-5α-(3,4-methylenedioxyphenyl)-dihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium methoxide, 2.) dil. sulfuric acid / 1.) benzene 2.) 4 h

2: 98 percent / H₂ / 10 percent Pd-C / ethyl acetate

With sulfuric acid; hydrogen; sodium methylate; palladium on activated charcoal; In ethyl acetate;