3-(2-Methoxyphenyl)-2-propynal

Base Information

Chemical Name:3-(2-Methoxyphenyl)-2-propynal
CAS No.:154884-63-6
Molecular Formula:C₁₀H₈O₂
Molecular Weight:160.172
Hs Code.:
DSSTox Substance ID:DTXSID001306471
Nikkaji Number:J1.252.685G

Synonyms:154884-63-6;SCHEMBL19475497;3-(2-Methoxyphenyl)-2-propynal;DTXSID001306471

Suppliers and Price of 3-(2-Methoxyphenyl)-2-propynal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-Methoxyphenyl)-2-propynal

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:160.052429494
Heavy Atom Count:12
Complexity:208

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:

Useful:

Canonical SMILES:COC1=CC=CC=C1C#CC=O

Technology Process of 3-(2-Methoxyphenyl)-2-propynal

There total 5 articles about 3-(2-Methoxyphenyl)-2-propynal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 767-91-9
1-ethynyl-2-methoxybenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 154884-63-6
3-(2-methoxyphenyl)propiolaldehyde

Guidance literature:: 1-ethynyl-2-methoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -40 ℃; for 0.25h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 1h;

With sodium dihydrogenphosphate; In tetrahydrofuran; hexane; tert-butyl methyl ether; water;
DOI:10.1021/ol3022287 DOI:10.1021/ol3022287