C₃₄H₂₉N₃O₅S

Base Information

• Chemical Name: C₃₄H₂₉N₃O₅S
• CAS No.: 1376947-98-6
• Molecular Formula: C₃₄H₂₉N₃O₅S
• Molecular Weight: 591.687
• Mol file: 1376947-98-6.mol

Synonyms:C₃₄H₂₉N₃O₅S

Chemical Property of C₃₄H₂₉N₃O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₉N₃O₅S

There total 5 articles about C₃₄H₂₉N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C33H27N3O3 (1376947-95-3) + methanesulfonyl chloride (124-63-0) → C34H29N3O5S (1376947-98-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 0.333333h;

DOI:10.1016/j.tet.2011.11.066

Reference yield:

N-ethoxycarbonylphthalimide (22509-74-6) → C34H29N3O5S (1376947-98-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium carbonate / water / 3 h

1.2: 0 - 20 °C

1.3: 2 h / 50 °C

2.1: sodium tetrahydroborate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.08 h / 0 °C

3.1: triethylamine / dichloromethane / 0.33 h / 0 °C

With sodium tetrahydroborate; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2011.11.066

Reference yield:

trityl chloride (76-83-5) → C34H29N3O5S (1376947-98-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium carbonate / water / 3 h

1.2: 0 - 20 °C

1.3: 2 h / 50 °C

2.1: sodium tetrahydroborate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.08 h / 0 °C

3.1: triethylamine / dichloromethane / 0.33 h / 0 °C

With sodium tetrahydroborate; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2011.11.066

upstream raw materials:

C₃₃H₂₅N₃O₄

C₃₃H₂₇N₃O₃

methanesulfonyl chloride

N-ethoxycarbonylphthalimide

Downstream raw materials:

C₃₃H₂₆N₆O₂