N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

Base Information

Chemical Name:N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc
CAS No.:851706-38-2
Molecular Formula:C₂₄H₃₅N₃O₆S₂
Molecular Weight:525.69
Hs Code.:

Synonyms:N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

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Chemical Property of N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

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Technology Process of N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

There total 5 articles about N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 851706-37-1
N-Boc-L-MeCys(Acm)-L-MeCys(Acm)-L-Pha-OAc

: 851706-38-2
N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

Guidance literature:: With iodine; In methanol; dichloromethane; at 25 ℃; for 12h;
DOI:10.3987/COM-04-10287

Reference yield:

: 851706-36-0
L-MeCys(Acm)-L-Pha-OAc

: 851706-38-2
N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 1-hydroxy-7-azabenzotriazole / dimethylformamide; CH₂Cl₂ / 12 h / 25 °C

2: 86 percent / iodine / CH₂Cl₂; methanol / 12 h / 25 °C

With 1-hydroxy-7-aza-benzotriazole; iodine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-04-10287

Reference yield:

: 851706-35-9
[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

: 851706-38-2
N-Boc-ox-[L-MeCys-L-MeCys]-L-Pha-OAc

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / TFA / CH₂Cl₂ / 3 h / 0 °C

2: 58 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 1-hydroxy-7-azabenzotriazole / dimethylformamide; CH₂Cl₂ / 12 h / 25 °C

3: 86 percent / iodine / CH₂Cl₂; methanol / 12 h / 25 °C

With 1-hydroxy-7-aza-benzotriazole; iodine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-04-10287